Section 2.4: Determination of Percent Ammonia For this procedure, the purpose was to determine the percent ammonia within our unknown synthesized compound. First, boric acid was dissolved inside of a flask that was then placed inside of a large beaker. For one solution, 0.3768 grams of the violet cobalt sample was incorporated into a separate flask along with solid sodium hydroxide. With the aid of glass tubing, the rubber stopper end of the tub sealed the flask containing the cobalt